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The operation of the filter reactor is suitable for temperature understanding

Date:2018/9/18Read:1434

       The filter reactor is suitable for laboratory/factory synthesis, catalysis or other solid-liquid chemical reactions and physical processes, so that one or more steps can be carried out in the same kettle body (such as suction filtration after the reaction is completed), thereby reducing the reaction bottom. The number of times the object is transferred, reducing the drift of the material measurement. Such as pharmaceutical, tobacco research and other fields. The strength of the glass is mainly determined by its surface condition, thickness and uniformity, and excessive surface stress causes damage to the device. Therefore, when handling glassware, avoid scratching the inside and outside of the surface and impact device. Thermal stress can cause damage. Avoiding rapid temperature changes and large internal and external temperature differences is important for protecting glass units. The external heating jacket and the internal reaction are strongly exothermic, and the cold bath can quickly pass into the hot reactor, which may cause the above consequences. The filtration reactor adopts a design of integrating the filtration membrane into the bottom of the tank, allowing the single or multi-step reaction process and the filtration process to be completed in the same kettle body, thereby reducing the number of transfer of the reaction materials, improving the experimental efficiency, and greatly reducing the efficiency. The loss of the reaction material and the cross-contamination of the filtration process. The filter is supported by a PTFE adapter with ACE SAFE threaded connection. The end of the thread has an O-ring. The inside of the reactor and the tray of the filter tray have special projections. The support of the filter is guaranteed to be available. The stable support underneath, the filtration efficiency is high, and there is no liquid leakage during filtration.
     The standard reactor has an operating temperature of up to 230 ° C and a temperature deviation of 80 ° C allowed inside and outside the kettle. When heating or cooling the reactor, it is recommended to continuously monitor the temperature inside and outside the kettle to avoid accidents. When using a heating mantle, care must be taken when the reactor is heated from room temperature to above 350 °C. If an adjustable temperature controller is used, it is recommended to use 3/4 of the voltage during the heating process and gradually increase the voltage until the temperature in the kettle reaches the set value without exceeding the internal and external temperature deviation.

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